The Book deals with first of all in Identification of type of research interested, Title formulation, hypotheses, Literature Review, Research Design and Methodology-Experimentation, Data collection, Analysis, interpretation and Discussion of the findings, Conclusions and Recommendations. Secondly, the book shows how to write Scientific reports, the major parts and what is to be included from beginning to the end, i.e. the title, abstract, introduction, statement of the problem, establishment of the knowledge gap, finding out what has already been done. Thirdly, it gives the techniques involved in scientific procedure and making the work attractive. The techniques of interest include the use of instrumentation and spectroscopic methods to determine the structures of starting materials and compare them with the products, checking the progress of reactions. Use of Thin Layer Chromatography or Gas Chromatography to determine the progress of the reactions and other techniques. References and useful appendices.